Experimental Data to the publication "Synthesis of Micro 14C-Labelled Polylactide for Environmental Assessment Analysis"

2026-07-01T00:16:07Zhttps://www.radar-service.eu/oai/OAIHandler

10.22000/ck37qkdet7mrfu3w2025-09-20T20:32:35Zradar4chem

10.22000/ck37qkdet7mrfu3w Adeleh, Sara Sara Adeleh Institute of Bio and Geosciences (IBG-3: Agrosphere), Forschungszentrum Jülich GmbH, 52425 Jülich, Germany, Institute of Inorganic Chemistry, RWTH Aachen University, Landoltweg 1A, 52074 Aachen, Germany and Bioeconomy Science Center (BioSC), Forschungszentrum Jülich GmbH, 52425 Jülich, Germany Becker, Tabea Tabea Becker 0009-0007-5243-1952 Institute of Inorganic Chemistry, RWTH Aachen University, Landoltweg 1A, 52074 Aachen, Germany, and Forschungszentrum Jülich GmbH, 52425 Jülich, Germany Herres-Pawlis, Sonja Sonja Herres-Pawlis 0000-0002-4354-4353 Institute of Inorganic Chemistry, RWTH Aachen University, Landoltweg 1A, 52074 Aachen, Germany, and Forschungszentrum Jülich GmbH, 52425 Jülich, Germany Bol, Roland Roland Bol 0000-0003-3015-7706 Institute of Bio and Geosciences (IBG-3: Agrosphere), Forschungszentrum Jülich GmbH, 52425 Jülich, Germany, and Bioeconomy Science Center (BioSC), Forschungszentrum Jülich GmbH, 52425 Jülich, Germany Drewes, Birte Birte Drewes 0000-0002-6849-1438 Institute of Neuroscience and Medicine (INM-5: Nuclear Chemistry) Forschungszentrum Jülich GmbH, 52425 Jülich, Germany Pütz, Thomas Thomas Pütz 0000-0003-2101-448X 1Institute of Bio and Geosciences (IBG-3: Agrosphere), Forschungszentrum Jülich GmbH, 52425 Jülich (Germany) and Bioeconomy Science Center (BioSC), Forschungszentrum Jülich GmbH, 52425 Jülich, Germany Experimental Data to the publication "Synthesis of Micro 14C-Labelled Polylactide for Environmental Assessment Analysis" RWTH Aachen University,Forschungszentrum Jülich 2024-2025 2025 Chemistry Materials Science 14C labeling NMR spectroscopy Size Exclusion chromatography lactide polymerization 14C-lactide and 14C-PLA NMR and IR spectroscopic data, SEC, TGA and DSC experimental data Open Access Creative Commons Attribution Non Commercial Share Alike 4.0 International RWTH Aachen University https://ror.org/04xfq0f34 Forschungszentrum Jülich https://ror.org/02nv7yv05 Further NMR and IR spectroscopic data, SEC data and TGA and DSC data for the ring opening polymerisation of 14C-lactide with a non toxic Zn catalyst were deposited. GPCmax VE-2001 from Viscotek: two Malvern Viscotek T columns (porous styrene divinylbenzene copolymer) with a maximum pore size of 500 and 5000Å, a refractive index detector (VE-3580), and a viscometer (Viscotek 270 Dual Detector) Bruker Avance II (400MHz) NMR spectrometer Bruker Avance III (400MHz) NMR spectrometer Shimadzu IRTracer 100 using a CsI beam splitter in combination with an ATR unit (Quest model from Specac utilizing a robust monolithic crystalline diamond) Netzsch DSC 204 F1 Phoenix equipped with an intra-cooler Linseis STA PT1600 with the HDSC Type S measuring unit (Pt10%/Pt-Rh) and the L75/240 RT-1600 furnace en Bioeconomy Science Center financially supported by the Ministry of Culture and Science BioSC 313/323-400-002 13 NRW Strategieprojekt BioSC BioPlastiCycle Werner Siemens-Stiftung WSS WSS-Jahrhundertprojekt catalaix application/x-tar