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    Dataset: Experimental Data to the publication "Synthesis of Micro 14C-Labelled Polylactide for Environmental Assessment Analysis"

    Alternate identifier:
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    Related identifier:
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    Creator/Author:
    Adeleh, Sara [Institute of Bio and Geosciences (IBG-3: Agrosphere), Forschungszentrum Jülich GmbH, 52425 Jülich, Germany, Institute of Inorganic Chemistry, RWTH Aachen University, Landoltweg 1A, 52074 Aachen, Germany and Bioeconomy Science Center (BioSC), Forschungszentrum Jülich GmbH, 52425 Jülich, Germany]

    Becker, Tabea https://orcid.org/0009-0007-5243-1952 [Institute of Inorganic Chemistry, RWTH Aachen University, Landoltweg 1A, 52074 Aachen, Germany, and Forschungszentrum Jülich GmbH, 52425 Jülich, Germany]

    Herres-Pawlis, Sonja https://orcid.org/0000-0002-4354-4353 [Institute of Inorganic Chemistry, RWTH Aachen University, Landoltweg 1A, 52074 Aachen, Germany, and Forschungszentrum Jülich GmbH, 52425 Jülich, Germany]

    Bol, Roland https://orcid.org/0000-0003-3015-7706 [Institute of Bio and Geosciences (IBG-3: Agrosphere), Forschungszentrum Jülich GmbH, 52425 Jülich, Germany, and Bioeconomy Science Center (BioSC), Forschungszentrum Jülich GmbH, 52425 Jülich, Germany]

    Drewes, Birte https://orcid.org/0000-0002-6849-1438 [Institute of Neuroscience and Medicine (INM-5: Nuclear Chemistry) Forschungszentrum Jülich GmbH, 52425 Jülich, Germany]

    Pütz, Thomas https://orcid.org/0000-0003-2101-448X [1Institute of Bio and Geosciences (IBG-3: Agrosphere), Forschungszentrum Jülich GmbH, 52425 Jülich (Germany) and Bioeconomy Science Center (BioSC), Forschungszentrum Jülich GmbH, 52425 Jülich, Germany]
    Contributors:
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    Title:
    Experimental Data to the publication "Synthesis of Micro 14C-Labelled Polylactide for Environmental Assessment Analysis"
    Additional titles:
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    Description:
    (Abstract) Further NMR and IR spectroscopic data, SEC data and TGA and DSC data for the ring opening polymerisation of 14C-lactide with a non toxic Zn catalyst were deposited.
    Keywords:
    14C labeling
    NMR spectroscopy
    Size Exclusion chromatography
    lactide polymerization
    14C-lactide and 14C-PLA
    Related information:
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    Language:
    English
    Publishers:
    RWTH Aachen University
    Forschungszentrum Jülich
    Production year:
    Subject areas:
    Chemistry
    Materials Science
    Resource type:
    (Dataset) NMR and IR spectroscopic data, SEC, TGA and DSC experimental data
    Data source:
    (Instrument) GPCmax VE-2001 from Viscotek: two Malvern Viscotek T columns (porous styrene divinylbenzene copolymer) with a maximum pore size of 500 and 5000Å, a refractive index detector (VE-3580), and a viscometer (Viscotek 270 Dual Detector)
    (Instrument) Bruker Avance II (400MHz) NMR spectrometer
    (Instrument) Bruker Avance III (400MHz) NMR spectrometer
    (Instrument) Shimadzu IRTracer 100 using a CsI beam splitter in combination with an ATR unit (Quest model from Specac utilizing a robust monolithic crystalline diamond)
    (Instrument) Netzsch DSC 204 F1 Phoenix equipped with an intra-cooler
    (Instrument) Linseis STA PT1600 with the HDSC Type S measuring unit (Pt10%/Pt-Rh) and the L75/240 RT-1600 furnace
    Software used:
    Resource processing
    Software:
    Omnisec - 5.12
    MestReNova - 14.2.3-29241
    Alternative software:
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    Software used:
    Resource production
    Software:
    TOPSPIN - 2.1
    TOPSPIN - 3.5 pl. 7
    Omnisec - 5.12
    LabSolution IR - 2.15
    NETZSCH Proteus – Thermal Analysis - 8.0.3
    Linseis TA Software - STA2
    TOPSPIN - 4.0.2
    TOPSPIN - 4.5.0
    Alternative software:
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    Data processing:
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    Publication year:
    Rights holders:
    Funding:
    Bioeconomy Science Center financially supported by the Ministry of Culture and Science - (NRW Strategieprojekt BioSC BioPlastiCycle)(313/323-400-002 13)
    Werner Siemens-Stiftung - (catalaix)(WSS-Jahrhundertprojekt)
    Name Storage Metadata Upload Action
    Status:
    Published
    Uploaded by:
    iac_Radar_Produktion
    Created on:
    Archiving date:
    2025-09-20
    Archive size:
    3.7 MB
    Archive creator:
    iac_Radar_Produktion
    Archive checksum:
    641c8a4829670691a24b391b8bf48fe4 (MD5)
    Embargo period:
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